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Tīmeklis2024. gada 15. okt. · A study of the strong N−X⋅⋅⋅ − O−N + (X=I, Br) halogen bonding interactions reports 2×27 donor×acceptor complexes of N-halosaccharins and pyridine N-oxides (PyNO). DFT calculations were used to investigate the X⋅⋅⋅O halogen bond (XB) interaction energies in 54 complexes. TīmeklisScheme 1. Synthesis of the gallium pyridyl nitroxide complex (pyNOº) 2GaCl (1) and the indium dimer [(pyNOº) 2In][(pyNOº) 2InCl 2] (2). 2.2. Structural Characterization Single crystals of the (pyNOº) 2GaCl complex were grown from a concentrated solution of diethyl ether at º25 °C. The molecule crystallizes in the orthorhombic space group Pna2 blackboard solutions
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